Examples of 'compound as a solid' in a sentence
Meaning of "compound as a solid"
compound as a solid - Refers to a chemical compound that is in a solid state, meaning its particles are closely packed together and have a definite shape and volume
How to use "compound as a solid" in a sentence
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compound as a solid
Purification gives the title compound as a solid.
Afterwards all volatiles are removed under reduced pressure to afford the title compound as a solid.
This yielded 100 mg of the title compound as a solid with a low melting point.
Subsequently the suspension is filtered to give title compound as a solid.
This provided the title compound as a solid.
The combined organic extracts are evaporated to yield the title compound as a solid.
This afforded the title compound as a solid.
The filtrate is concentrated and purified to give the title compound as a solid.
The solid collected was dried to provide the title compound as a solid contaminated by ca.
Purification of the residue by silica gel chromatography afforded the title compound as a solid.
Lyophilize the mixture to afford the title compound as a solid.
The method of claim 1, further comprising isolating the monocyclopentadienyl compound as a solid.
Chromatography on silica gel gave the title compound as a solid.
After filtration and concentration, purification by column chromatography afforded the title compound as a solid.
Recovered 55 mg of the title compound as a solid.
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Elution with dichloromethane initially, grading to 5 % methanol-dichloromethane provided the title compound as a solid.
This afforded 2.4 g of the title compound as a solid.
Afterwards all volatiles were removed to give the title compound as a solid.
This gives 406 mg of the title compound as a solid.
The resulting mixture is filtered to obtain the desired compound as a solid.
Drying under vacuum afforded the title compound as a solid.
The solvent is removed in vacuo to yield the title compound as a solid.
The resulting suspension is filtered to afford the title compound as a solid.
The resulting solution was filtered to obtain the title compound as a solid.
The mixture was freeze dried to give the title compound as a solid.
Evaporation of the desired fractions afforded the title compound as a solid.
Concentration of the organic extracts yields the title compound as a solid.
The solution was evaporated in vacuo to yield the title compound as a solid.
The volatiles were removed under vacuo to give the title compound as a solid.
All volatile materials are removed in vacuo to give the title compound as a solid.
Evaporate the product containing fractions to give the title compound as a solid.
The procedure is repeated a second time to afford the title compound as a solid.
Recrystallize the residue from diethyl ether to give the title compound as a solid.
The present invention further provides a method of isolating the desired compound as a solid.
Filtration and subsequent drying of the precipitate afforded the title compound as a solid.
All such fractions were combined and evaporated to yield the title compound as a solid.
The crude oil was purified by flash chromatography to yield the tittle compound as a solid.
Diethyl ether was added and the gum triturated to give the titled compound as a solid.
The resulting precipitate is filtered off and dried to afford the title compound as a solid.
The mixture was treated with water and filtered to provide the title compound as a solid.
The mixture was treated with water and filtered to provide the tittle compound as a solid.
Evaporation of the solvent gave 2mg of the title compound as a solid.
Evaporation in vacuo from hexane / dichloromethane gives the title compound as a solid.
This dissolution / evaporation procedure was repeated to give the title compound as a solid.
Triturate with hexane, filter and dry in vacuo to give the title compound as a solid.
The solid was re-crystallized from DCM to yield the title compound as a solid.
The fractions were distilled to give 80 mg of desired compound as a solid.
Chromatography ( silica gel ) afforded the title compound as a solid.
The solvent was evaporated to give 46 g of the titled compound as a solid.
Eluting with methylene chloride to provide 116 g of the title compound as a solid.
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