Examples of 'crystalline residue' in a sentence
Meaning of "crystalline residue"
crystalline residue: a deposit or layer of small, sparkling particles left behind after evaporation or crystallization
How to use "crystalline residue" in a sentence
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crystalline residue
The crystalline residue is dissolved in anhydrous methanol.
Evaporation of the solvent leaves a crystalline residue.
The remaining crystalline residue was dried in vacuum.
The filtrate was concentrated to give a crystalline residue.
The crystalline residue was purified by flash chromatography.
The filtrate was concentrated to obtain a crystalline residue.
The crystalline residue was recrystallized from ethanol.
The filtrate evaporated to dryniss gives a crystalline residue.
The crystalline residue was triturated with hexane.
Evaporation to dryness gave a crystalline residue.
The crystalline residue is recrystallized from acetonitrile.
Removal of solvent gave a crystalline residue.
The crystalline residue is digested with diethyl ether.
It is then evaporated and the crystalline residue is recrystallized from toluene.
The crystalline residue is dried by azeotropic distillation with toluene.
See also
The ethyl acetate layer was concentrated to obtain the crystalline residue.
Means the efflorescent crystalline residue we are looking at is atropine trace.
Filtered and the filtrate concentrated in vacuo to give a crystalline residue.
A crystalline residue from this digestion was found to be ammonium perthiocarbonate.
The ethanol was removed in vacuo and the crystalline residue was collected by filtration.
The crystalline residue is partitioned between methylene chloride and water.
The catalyst was filtered off and the solution was concentrated to a crystalline residue.
The hygroscopic crystalline residue obtained after evapouration is the desired product in its trifluoracetic form.
The extract was dried and the solvent removed to leave a crystalline residue.
The pale yellow crystalline residue corresponds to hydrate form E.
The AcOEt was distilled off and hexane was added to the crystalline residue.
A yellow-white crystalline residue was obtained.
The ether was then distilled off under reduced pressure to give a crystalline residue.
The crystalline residue is taken up in water, ethyl acetate and aqueous ammonia solution.
This procedure was repeated until the water was removed and a crystalline residue remained.
The crystalline residue is washed with petroleum ether and 35 g of crystals are collected after filtration.
The solvent was evaporated in vacuo and the crystalline residue was washed with cold ether.
The obtained colourless emulsion was concentrated at normal pressure to leave a light brown crystalline residue.
The crystalline residue is triturated with ethanol, filtered by suction and washed with cold ethanol.
The compositions of the present invention do not leave a crystalline residue on the substrate surface.
The crystalline residue is triturated with 10 mL of ether.
Upon filtration, the filtrate was concentrated under reduced pressure to give a crystalline residue.
Solvent was removed by rotary evaporation, and the crystalline residue recrystallized from ethyl acetate / heptane.
Dry toluene was added to the residue and then evaporated, leaving a crystalline residue.
The crystalline residue is suspended in 70 ml of acetone.
After filtration and evaporation of the filtrate, the crystalline residue is washed with petroleum ether.
The crystalline residue was recrystallized from ethanol / isopropyl ether, giving 5.4 g of pale yellow crystals.
Dry EtOAc extract with Na ₂ SO ₄ and evaporate to dryness to provide a crystalline residue.
The resulting crystalline residue was homogenized in a blender using a 3:1 mixture of ether and petroleum ether.
The organic layer was concentrated to give 726 mg of crystalline residue.
This gave a crystalline residue of the crude product, which was recrystallized in methanol, M. p.
The toluene solution is evaporated under vacuum to obtain a crystalline residue of 47.5 g.
The partially crystalline residue was triturated with ethyl acetate ( 50 mL ).
The organic phases were combined and slowly concentrated at 60°C to provide a crystalline residue.
Solvent was removed, and the crystalline residue suspended in toluene ( 50 mL ).
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