Examples of 'crystallization solvent' in a sentence
Meaning of "crystallization solvent"
crystallization solvent: Refers to a substance in which a solute can be dissolved to form crystals during the process of crystallization, commonly used in chemistry and material sciences
How to use "crystallization solvent" in a sentence
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crystallization solvent
The crystallization solvent is only pure water.
The methanol typically is donated by crystallization solvent.
An example of a crystallization solvent is a mixture of acetonitrile and water.
Of residual methanol as the crystallization solvent.
A typical crystallization solvent is water.
The filtration cake is washed with the crystallization solvent.
The mixture was heated and crystallization solvent was added to obtain a clear solution.
The crystals were filtered and washed with fresh crystallization solvent.
Of residual crystallization solvent.
The method may further comprise crystallizing the montelukast acid from a crystallization solvent.
The crystallization solvent can be a single solvent or a mixed solvent comprising the solvents mentioned above.
The crude IPA may then be further purified by recrystallizihg in another selective crystallization solvent.
Preferably, crystallization solvent is a mixture of acetone and water.
The process of claim 1 wherein the crystallization solvent is toluene.
Typically, a crystallization solvent can be selected from isopropanol, ethyl acetate or an acetonitrile / water mixture.
See also
However, it has been found to dry slowly and to retain crystallization solvent.
In a preferred embodiment, crystallization solvent is a mixture of acetone and water.
Suitable co-solvents include the same solvents as identified above for the crystallization solvent.
A process as claimed in claim 7, wherein the crystallization solvent is a mixture of ethanol and water.
In another embodiment, the process further comprises crystallizing the montelukast acid from a crystallization solvent.
Further, the co-solvent and the crystallization solvent may be the same or different.
The purified amorphous compound of formula ( I ) is crystallized by selecting water as a crystallization solvent.
In a particular aspect of the invention, the crystallization solvent in step iii is ethyl acetate.
The crystallization solvent is any solvent or cosolvent mixture in which compound ( 1 ) will dissolve.
If desired, one or more further recrystallizations from the crystallization solvent may be effected.
Optionally, the crystallization solvent can be cooled after step ( b ).
Redissolving said separated purified TPA in a selective crystallization solvent to form a second solution ;.
The pure product contains less than 20 p . p.m. of residual methanol as the crystallization solvent.
The process of claim 1 wherein the crystallization solvent in step d is ethanol or 1-butanol.
A mixture of ethyl acetate, ethanol 9:1 was used as the crystallization solvent.
The method according to claim 6, the crystallization solvent is a mixture of methylene chloride and n-Hexane.
Preferably 1-butanol or ethanol is used as a crystallization solvent.
Redissolving crude IPA in a selective crystallization solvent at a temperature from 50°C to 250°C to form a second solution ;.
The screening examined acid type, acid level ( equivalents ), and / or type of crystallization solvent.
The method according to claim 2, wherein the crystallization solvent is a mixed solvent of ethanol / water.
Polymorph Form III may be prepared by crystallization from a crystallization solvent containing Compound 1.
The preferred carbon-treatment / crystallization solvent is methanol.
A process as claimed in claim 8, wherein the crystallization solvent is water.
In the case of FIG . 29, the crystallization solvent is pure methanol.
The process of claim 35, wherein the crystallization solvent is heptane.
In the case of FIG . 28, the crystallization solvent is pure water.
Compound ( 3 ) is dissolved in the above Crystallization Solvent with heating.
Compound ( I ) appearance crystallization solvent.
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