Examples of 'distillation under reduced' in a sentence
Meaning of "distillation under reduced"
The phrase 'distillation under reduced' refers to the process of distilling or separating substances by applying reduced pressure or vacuum conditions. It is commonly used in scientific or technical contexts, particularly in chemistry and laboratory settings, to describe the distillation technique where pressure is intentionally lowered to facilitate the separation of volatile components from a mixture
How to use "distillation under reduced" in a sentence
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distillation under reduced
Toluene was removed by distillation under reduced pressure.
The distillation under reduced pressure resulted in the unsymmetrically substituted malonic acid diethylester.
Water was removed by distillation under reduced pressure.
The oil component is separated into a refined distillate and a residuum by distillation under reduced pressure.
The solvents are removed by distillation under reduced pressure on a rotary evaporator.
Typically the trifluoroacetic acid is removed by azeotropic distillation under reduced pressure.
Methanol was removed by distillation under reduced pressure to afford yellow oil.
This mixture is subsequently subjected to fractional distillation under reduced pressure.
The solvent was removed by distillation under reduced pressure to eliminate volatile components.
Examples of purification include chromatography or distillation under reduced pressure.
The solvent is removed by distillation under reduced pressure in order to obtain crude product.
The amides could be purified by crystallization or distillation under reduced pressure.
The solvent was removed by distillation under reduced pressure and added thereto was dichloromethane.
Thereafter the desired anhydride was purified by distillation under reduced pressure.
Evaporation and distillation under reduced pressure was performed to eliminate Et3SiO.
See also
distillation techniques
distillation tower
distillation under reduced pressure
distillation under vacuum
The final product is recovered by distillation under reduced pressure.
After distillation under reduced pressure the pH was adjusted to 5 using hydrochloric acid.
Ethylacetate was removed by distillation under reduced pressure.
After distillation under reduced pressure, an oil corresponding to the title product is obtained.
Tetrahydrofuran was removed by distillation under reduced pressure.
Preferably, the distillation under reduced pressure is carried out under the protection of nitrogen gas.
The filtrate is concentrated by distillation under reduced pressure.
Distillation under reduced pressure gave the desired nitrile with a yield of 45 %.
Remove the toluene by distillation under reduced pressure.
The polyorganosilylated carboxylate compound of formula ( I ) can be isolated by distillation under reduced pressure.
The toluene was then removed by distillation under reduced pressure at room temperature.
Following several hours of incubation all volatiles were removed vÃa distillation under reduced pressure.
The solvent was removed by distillation under reduced pressure provided by a water aspirator.
This purification usually consists in carrying out a distillation under reduced pressure.
The solvent was removed by distillation under reduced pressure, which gave an active ester compound.
The remaining methyl salicylate is removed vÃa distillation under reduced pressure.
The solvent was removed by distillation under reduced pressure to yield a viscous, orange / yellow coloured liquid.
Two liters of tetrahydrofuran were removed by distillation under reduced pressure.
Distillation under reduced pressure ( 10 mbar ) afforded the desired compound as colorless liquid.
The residue is purified by distillation under reduced pressure.
After 1 h, distillation under reduced pressure was carried out to evaporate THF.
The solvent is eliminated by distillation under reduced pressure.
After distillation under reduced pressure, 5-mehyl-caproic acid was obtained.
The solvent is removed by distillation under reduced pressure.
Distillation under reduced pressure afforded the diethyl 2 ( w-bromoalkyl ) malonate.
The derivative is isolated by distillation under reduced pressure.
The purification process is carried out conventionally by multistage distillation under reduced pressure.
The latter was subjected to distillation under reduced pressure using a spinning band column.
The filtrate and the wash waters were concentrated by distillation under reduced pressure.
After removing tetrahydrofuran by distillation under reduced pressure, the organic layer is extracted with ether.
The solvent and excess benzoyl chloride were eliminated by distillation under reduced pressure.
The filtrate was subjected to distillation under reduced pressure to remove therefrom the solvent.
Much of the excess acetic anhydride was then removed by distillation under reduced pressure.
One portion was concentrated by distillation under reduced pressure to a residual volume of about 60ml.
The acetonitrile and the excess phosphorous trichloride are removed by distillation under reduced pressure.
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Examples of using Reduced
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The original should be reduced as little as possible
Reduced throughput time from production to delivery
Border delays must be reduced as much as possible