Examples of 'drying in vacuo' in a sentence
Meaning of "drying in vacuo"
Drying in vacuo: Refers to the process of drying a substance or material in a vacuum environment to remove moisture or other volatile components without oxidation or contamination
How to use "drying in vacuo" in a sentence
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drying in vacuo
Drying in vacuo gave a white solid product.
Evaporation of solvents and drying in vacuo resulted in an oil.
Drying in vacuo yields the crude product.
The product is obtained in crystalline form after drying in vacuo.
After drying in vacuo the polymer takes on a white colour.
The expected product is isolated by filtration and drying in vacuo.
After drying in vacuo the title compound is obtained as a yellow solid.
The title compound was isolated by concentration and drying in vacuo.
Evaporation of the volatiles and drying in vacuo afforded the final products.
A pure orange compound was obtained after filtration and drying in vacuo.
This was followed by filtration and drying in vacuo to give white crystals.
The material was further purified by washing with methanol and drying in vacuo.
Evaporation of the purified fractions and drying in vacuo afforded the title compound.
The desired title compound was obtained as a solid after filtration and drying in vacuo.
Filtration of the suspension and drying in vacuo gives the title compound as white solid.
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The title compound is obtained in pure form after drying in vacuo.
Re-evaporation and drying in vacuo affords the desired product.
The polymer was isolated by filtration and washed with methanol before drying in vacuo.
Liquors were removed after drying in vacuo for about 5 minutes.
The isolated crude product was used in the next reaction step after drying in vacuo.
Filtration and drying in vacuo afford the desired product as slightly brownish short needles, m . p.
A3 is then isolated by filtration and drying in vacuo.
On drying in vacuo at 40 oC overnight, the product hardened to a glass.
The crystals were collected by filtration, followed by drying in vacuo.
Liquors were removed by drying in vacuo for about 10 minutes.
The precipitate is centrifuged, triturated in ether and centrifuged again, followed by drying in vacuo.
Drying in vacuo afforded 10 mg the title compound as a red solid.
The product was isolated by precipitation with ethyl acetate, filtration and drying in vacuo.
After filtering and drying in vacuo 150 mg of the complex was isolated.
A white powder was obtained after repeated washings with n-hexane and drying in vacuo.
Rotary evaporation followed by further drying in vacuo have 431 mg of the desired product.
A yellowish brown solid was isolated by centrifugation, washing with pentane and drying in vacuo.
Concentration and drying in vacuo overnight yielded the ethanedioate salt ( 38 mg ) as a white gum.
The polymer mass was isolated by precipitating with methanol, washing and drying in vacuo.
After filtration and drying in vacuo at 50°C a white powdery material was recuperated.
A generated crystal was collected by filtration and washed with water, followed by drying in vacuo.
After filtration and drying in vacuo at 60 °C the title compound is obtained as a solid.
The crystals were collected by filtration to yield 3.5 g after drying in vacuo.
Drying in vacuo gave 31 g of solid.
The filtercake was washed with cold water before drying in vacuo at 60°C.
After drying in vacuo overnight, 167 mg of the title compound was obtained.
Evaporation of the purified fractions and drying in vacuo afforded 26.36 g of the title compound.
After drying in vacuo 0.45 g of the title compound was obtained as a white solid.
After filtration over a frit and drying in vacuo at 50 ° C., the desired product is obtained.
Drying in vacuo over phosphorus pentoxide gave 7.65 g of an impure white solid.
Trituration with ether, filtration and drying in vacuo afforded the crude product as a white solid ( 9.3 g ).
Drying in vacuo results in the title compounds ( final compounds 1-3 ) as colorless solids.
Filtration and drying in vacuo give 2,6-diethylphenyl boronic acid as a white solid.
Drying in vacuo at 40 °C for 2 days afforded the title compound.
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