Examples of 'give compound' in a sentence
Meaning of "give compound"
Give compound: Likely a typo; unclear meaning. Please provide more context for an accurate definition
How to use "give compound" in a sentence
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give compound
Then the organic solvent was removed to give compound XX.
The filtrate was concentrated to give compound 9B for next reaction without further purification.
Then the organic solvent was removed to give compound XIX.
The protection of a-carboxyl group to give compound 10 with trichloroethanol is accomplished according to Scheme 6.
The solids may be collected from this dilution and dried to give compound VI.
The filtrate was concentrated to give Compound AL without further purification.
The solid thus obtained was washed with a aqueous methanol and dried to give compound V.
Reacting to give compound IV.
The dark green solution was separated by suction filtration and then lyophilized to give compound W.
The solution was concentrated to dryness, to give compound 3 in the form of a yellow oil.
The mixture was concentrated and purified by column chromatogram to give compound 5.
The resulting slurry was filtered to give compound 26 as a crude product.
Compound 1 was further alkylated using dibromoethane at high temperature to give compound 3.
The precipitate is collected by filtration to give compound 4 with very little impurity.
The precipitate was recrystallized from methylene chloride by addition of methanol to give compound 8.
See also
The intermediate reacts with known compound 6 to give compound 7 of the present application.
As shown in Scheme 1, compound a undergoes a stereoselective decarboxylation to give compound b.
Compound XXXVa reacted with diphenyl cyanocarbonimidate to give compound 37 and with sulfamide to give compound 38.
The double bonds may be hydrogenated using a catalyst such as platinum to give compound 16.
The final product was purified by RP-HPLC to give compound 20 as a white powder after lyophilization.
The mixture was diluted with acetonitrile and purified by HPLC to give Compound No.
To give compound 4.
The solvents were evaporated to give compound XVII.
This is the step to give Compound 20 by azidation of Compound 19.
Compound LA can also react with ketone or aldehyde to give compound of Formula IL.
The residue was chromatographed on a column of silica gel to give compound 3.
The crude product is recrystallized from heptane to give compound I in 58 to 67 % yield . Catalytic hydrogenation.
The intermediate is heated to carry out cyclization to give compound 5.
The product is purified by column chromatography to give Compound 1D as an off-white solid.
The suspension was filtered and the organic phase was concentrated to give compound 17.
The product is dried to give Compound II.
The reaction mixture was concentrated and purified by prep-HPLC to give compound 5.
The organics were concentrated in vacuo to give compound 3 as waxy solid.
Solvent and excess reagent was removed under reduced pressure to give compound 16.
The organic phase was concentrated in vacuo to give compound 2 as colorless oil.
The protecting group is removed under acidic conditions in an organic solvent to give compound 27.
Compound I-a was then decarboxylated to give compound I-b of this invention.
The residue is chromatographed over silica gel with ethyl acetate / hexane to give compound 9.
The hydroxyl-protecting group is removed to give compound ( 1 ) of the present invention.
Thus obtained Compound 7 is treated with a base in a suitable solvent to give Compound 8.
The melted solids were stirred overnight to give compound 438 as a yellow-brown solid.
After the mixture was allowed to cool, precipitated crystals were filtered to give Compound c1.
After filtration, the filtrate was concentrated to give compound as a white solid.
The appropriate fractions are then desalted by reverse-phase chromatography to give Compound 5.
The mixture was concentrated and dried in vacuo to give Compound 1j as a TFA salt.
Introduction of the moiety A7 may be accomplished as described for step a to give compound 6.
HCl dropwise . The resulting solution was lyophilized to give Compound 1e as a light yellow solid.
This compound can then undergo displacement with acetate anion to give compound 6.
The organic layer was concentrated to give compound of formula ( II ).
The isopropylidene group could then be removed under acidic conditions to give compound 13b.
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