Examples of 'reflux under nitrogen' in a sentence

Meaning of "reflux under nitrogen"

reflux under nitrogen: This phrase pertains to a chemical process involving the distillation of a substance under a nitrogen atmosphere to prevent oxidation

How to use "reflux under nitrogen" in a sentence

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reflux under nitrogen
The mixture was heated to reflux under nitrogen.
Heat at reflux under nitrogen for twenty hours.
The contents were heated to reflux under nitrogen.
Heat at reflux under nitrogen for three hours.
The reaction is heated to reflux under nitrogen.
Stirring at reflux under nitrogen was continued until all of the solid had dissolved.
The reaction was heated to reflux under nitrogen.
Stir and reflux under nitrogen for 30 minutes.
The mixture was stirred at reflux under nitrogen.
Heat the mixture under reflux under nitrogen atmosphere overnight.
The mixture was heated with stirring to reflux under nitrogen.
The mixture was stirred at reflux under nitrogen with constant water removal.
This mixture was agitated and heated to reflux under nitrogen.
The filtrate was heated to reflux under nitrogen atmosphere to strip the solvent.
The resulting solution was stirred at reflux under nitrogen.

See also

The mixture is boiled under reflux under nitrogen with vigorous stirring for 5 hours.
The suspension was stirred magnetically and brought to reflux under nitrogen.
Heat the mixture at reflux under nitrogen overnight.
The reaction is purged with nitrogen three times and heated to reflux under nitrogen.
The reaction is heated to reflux under nitrogen and monitored by TLC.
The sparging was stopped, and the flask was heated at reflux under nitrogen.
The reaction was heated to reflux under nitrogen and monitored by TLC.
Dissolving a compound described by structure 6, in dry benzene and heating it to reflux under nitrogen.
The mixture was heated at reflux under nitrogen overnight.
Mercuric acetate ( Hg ( OOCCH3 ) 2 ) is added and the reaction is heated to reflux under nitrogen.
The mixture is heated to reflux under nitrogen and monitored by HPLC.
The reaction was left further 24 hours with reflux under nitrogen.
Heat the mixture under reflux under nitrogen atmosphere for 4 h.
Concentrated HCl ( ca 3 drops ) was added and the reaction heated to reflux under nitrogen.
It was then heated to reflux under nitrogen for 5 hours.
Concentrated HCl ( 0.5 mL ) was added and the reaction heated to reflux under nitrogen.
Heat the mixture to reflux under nitrogen for 2 hours.
Concentrated HCl ( 0.5 mL ) is added and the reaction heated to reflux under nitrogen.
The mixture is stirred at reflux under nitrogen for 2 hours.
After addition, the resulting mixture was stirred at reflux under nitrogen for 3 h.
The solution was kept at reflux under nitrogen for 11 hrs, then was evaporated.
To the mixture is added 14E and the reaction is heated to reflux under nitrogen overnight.
The mixture is heated at reflux under nitrogen for 24 hours with stirring.
Hydrochloric acid ( 2ml ) was added and the mixture was heated at reflux under nitrogen for 18h.
The mixture was heated at reflux under nitrogen over the weekend ( for about 72 h ).
The mixture is then heated at reflux under nitrogen.
The mixture was then heated at reflux under nitrogen until the reaction is complete ( 8-45 hrs ).
The solvent was heated to gentle reflux under nitrogen.
Heat the reaction to reflux under nitrogen for 3 hours.
After addition, the reaction mixture was heated at reflux under nitrogen for 6 days.
The solution is then brought to reflux under nitrogen atmosphere.
The resulting pale yellow solution was heated at reflux under nitrogen for 3.5 h.
Fit with condenser and heat at reflux under nitrogen overnight.
Stir and slowly heat to reflux under nitrogen.
The brown reaction mixture was heated to reflux under nitrogen and turned yellow.

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Examples of using Nitrogen
Tackling nitrogen pollution and biodiversity loss
Produces oxides of sulphur and nitrogen on combustion
Workshop on nitrogen processes and dynamic modelling
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Examples of using Reflux
I got acid reflux like something severe
This could just be a case of gastro reflux
Reflux of gastric juice into the gullet
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