Examples of 'crude intermediate' in a sentence
Meaning of "crude intermediate"
crude intermediate - refers to a basic or rudimentary stage in between progress
How to use "crude intermediate" in a sentence
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crude intermediate
The crude intermediate azide was not characterized.
Filtration and concentration afforded the crude intermediate.
This crude intermediate was used as such in the next step.
The filtrate was evaporated to afford the crude intermediate.
This crude intermediate may be hydrogenated without further purification.
The mixture was evaporated in vacuum to give the crude intermediate.
The crude intermediate imine was separated by evaporation and reduced as described above.
The acetonitrile was removed under vacuum and the crude intermediate precipitates were collected by filtration.
This crude intermediate was used directly for the next reaction step.
The combined filtrate and washing portion was concentrated in vacuum to afford the crude intermediate.
The HCl in the crude intermediate stream is recovered using an HCl column.
After filtration, the concentrated filtrate under reduce pressure gave a brown syrupy crude intermediate 5.
The crude intermediate was purified via flash chromatography using DCM and MeOH as eluents.
After concentration, the crude intermediate was obtained.
Crude intermediate 1 was used without further purification.
See also
Evaporation of the combined product fractions provided crude intermediate 42, which was triturated with diisopropyl ether.
The crude intermediate was not purified, and was carried on to the next step.
Cc of 1N HCl was added to this crude intermediate to obtain a mixture.
Gave the crude intermediate isocyanate which was used in step 7, below without purification.
The organic phase was concentrated by evaporation and dried to yield crude Intermediate 4.
This crude intermediate was dissolved as such in 1N HCl to obtain a solution.
The organic phase was concentrated and dried to give the crude Intermediate 6.
This crude intermediate was dissolved as such in 1N HCI to obtain a solution.
Cc of 1 N HCI was added to this crude intermediate to obtain a mixture.
The above crude intermediate was dissolved in dichloromethane ( 5 mL ).
Residue was triturated with methanol to give 6.5 g of crude intermediate.
The crude intermediate 33 was used in the next reaction without purification.
Residue was trituated with methanol to give 6.5 g of crude intermediate.
The crude intermediate 34 is used in the next reaction without purification.
The appropriate fraction was evaporated to give the required crude intermediate ( 2 g ).
Dissolve the crude intermediate in dioxane ( 5 mL ) and purge with nitrogen.
Solution, followed by drying and concentration to give 340 mg of the crude intermediate product.
The crude intermediate nitrile was purified by flash chromatography ( hexane / EtOAc ) chromatography.
Remove the solvent under vacuum then dissolve the crude intermediate in acetic acid ( 20 mL ).
This crude intermediate was dissolved at room temperature in 50 ml of DMF.
The filtrate was evaporated to give crude Intermediate 6 ( 8 g ) which was used without purification.
Air was then bubbled through the solution overnight at 55°C to form the crude intermediate.
After cooling to room temperature, the crude intermediate was stirred with 1 N hydrochloric acid for 3 hours.
Crude Intermediate 10B was carried onto the next step.
After filtration of the N, N ' - dicyclohexylurea, the crude intermediate product has been precipitated with water.
The crude intermediate alcohol was immediately dissolved in 2 mL of 1,2-dichloroethane.
Removal of solvent afforded 100 mg of crude intermediate.
The crude intermediate ester was separated by extracting with dichloromethane ( 3 x 50 ml ).
After evaporation of the solvent 4.95 g of crude intermediate 1 were obtained.
This crude intermediate was dissolved in dry dichloromethane ( 20 mL ) under argon.
The combined organic layers were concentrated in vacuo, yielding crude intermediate silylether ( 11 g ).
The crude intermediate was purified by silica gel chromatography ( MeOH/EtOAc/Et3N ).
The organic layer was evaporated to dryness to yield crude Intermediate ( 10a ).
Crude Intermediate 2-5 was used as such in the next step ( no yield was determined ).
After removal of the solvent under reduced pressure, a second bath of crude Intermediate 26-2 was obtained.
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Obtain intermediate result of addition and subtraction
Toluenediamine is formed as an intermediate product in the reaction
An intermediate flame size is used to continue cooking
Examples of using Crude
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Merely a very crude attempt at lending privacy
Crude things about their intimate relationship
Extraction of crude petroleum and natural gas
