Examples of 'methanol in dichloromethane' in a sentence
Meaning of "methanol in dichloromethane"
methanol in dichloromethane - Refers to a chemical solution or mixture containing methanol and dichloromethane as solvents or components
How to use "methanol in dichloromethane" in a sentence
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methanol in dichloromethane
The column was eluted with increasing amounts of methanol in dichloromethane.
Elute with 1 % methanol in dichloromethane and concentrate in vacuo to obtain a foam.
This solid was again triturated with a small amount of methanol in dichloromethane.
Elution with 5 % methanol in dichloromethane provided the title compound as a yellow oil.
The solution was adsorbed onto silica and eluted using methanol in dichloromethane.
To the residue was added 5 % methanol in dichloromethane and the insoluble solid removed by filtration.
The resulting oil was chromatographed over silica gel eluting with methanol in dichloromethane.
Chromatography on silica eluting with 4 % methanol in dichloromethane gave the title product as an oil.
The crude residue was subjected to flash column chromatography with 2 % methanol in dichloromethane.
Column chromatography eluting with 4 % methanol in dichloromethane gave the desired product.
The reaction mixture was passed through a short silica plug and washed with 5 % methanol in dichloromethane.
Then elution with 5 % methanol in dichloromethane and recrystallisation from toluene yields the pure final product.
The residue was subjected to chromatography using 2 % methanol in dichloromethane as eluant.
Elution with 5 % methanol in dichloromethane containing 1 % conc.
The residue is purified on a silica column with a 2 % mixture of methanol in dichloromethane.
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To this solid is added 10 % methanol in dichloromethane and sodium sulfate.
This crude was purified by flash chromatography eluting with 2 % methanol in dichloromethane.
The compound was eluted in 2 % methanol in dichloromethane as pale yellow colour solid title compound 69.
The product was purified on a silica column using a dichloromethane to 5 % methanol in dichloromethane gradient.
Concentrate the solution, dissolve in 5 % methanol in dichloromethane and purify through a short silica gel plug.
The residue was applied to a silica column and eluted with 2 % methanol in dichloromethane.
This oil was eluted with 10 % methanol in dichloromethane through silica vÃa HPLC to yield 7 g oil.
The residue was purified vÃa column chromatography using a dichloromethane to 5 % methanol in dichloromethane gradient.
Elution with 1-2 % methanol in dichloromethane afforded a green / brown solid.
The crude mixture is purified by chromatography using 2 % methanol in dichloromethane as a solvent system.
Purification of the crude product was achieved by column chromatography, eluting with 10 % methanol in dichloromethane.
The resin was finally washed with 10 % methanol in dichloromethane and vacuum dried.
The crude mixture was purified by flash chromatography eluting the product with 5-15 % methanol in dichloromethane.
This reaction mixture was dissolved in 50 % methanol in dichloromethane and pre-adsorbed onto silica.
The residue is purified by chromatography using a gradient of 0 to 10 % of methanol in dichloromethane.
Chromatography on silica gel with 5 % methanol in dichloromethane gave 100 mg of pure product.
The silica gel was eluted first with dichloromethane then with 5 % methanol in dichloromethane.
Column chromatography with 5 % methanol in dichloromethane gives the compound in > 30 % overall yield.
The crude was purified vÃa silica gel chromatography using a dichloromethane to 10 % methanol in dichloromethane gradient.
The column was eluted with 5 % methanol in dichloromethane and then with 10 % methanol in dichloromethane.
The residual oil was purified by medium pressure chromatography using 5 % methanol in dichloromethane as eluent.
Chromatography on silica eluting with 2 % methanol in dichloromethane gave a yellow oil.
This material was purified by chromatography eluting with 10 % methanol in dichloromethane.
The yield after preparative TLC 5 % methanol in dichloromethane was 4 mg.
Purification was by biotage chromatography on silica eluting with 2-5 % methanol in dichloromethane.
The product eluted out at 12 % methanol in dichloromethane.
The oil was purified on silica gel eluting with a gradient of 0 to 7 % methanol in dichloromethane.
The solid was washed with 20 % methanol in dichloromethane.
The fritted funnels from the previous filtrations were rinsed with a 50 % mixture of methanol in dichloromethane.
Solids were washed with 20 % methanol in dichloromethane.
The resulting solid was purified by silica gel column chromatography eluting with 0.5 % methanol in dichloromethane.
Purification by column chromatography, on gradient elution with methanol in dichloromethane ( 5 to 15 % ), afforded a glass.
The product was repurified by flash chromatography, eluting 1 % ammonium hydroxide 10 % methanol in dichloromethane.
Purification by silica gel chromatography using 10 % methanol in dichloromethane afforded 40 mg XI.
The plate was eluted with dichloromethane, followed by a gradient of 0.5 % to 2 % methanol in dichloromethane.
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Examples of using Dichloromethane
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The dichloromethane was evaporated under reduced pressure
The total quantity of dichloromethane loaded is unchanged
Dichloromethane and water were added to the residue
Examples of using Methanol
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Methanol will not persist in the environment
Five litres of methanol five weeks ago
Methanol can be used to create scents or aromas
