Examples of 'methanol in ethyl' in a sentence
Meaning of "methanol in ethyl"
methanol in ethyl - possibly referring to a chemical process or mixture involving the substances methanol and ethyl
How to use "methanol in ethyl" in a sentence
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methanol in ethyl
The residue was chromatographed on alumina with 5 % methanol in ethyl acetate as eluant.
Purification by flash chromatography ( 7 % methanol in ethyl acetate ) afforded the free piperazine as a white solid.
Purification was by flash column chromatography eluting with 5 % methanol in ethyl acetate.
Purification by flash chromatography ( 2 % methanol in ethyl acetate ) afforded the alkylated compound as a white solid.
The residue was then dissolved in a minimal amount of hot 5 % methanol in ethyl acetate.
Purification by preparative TLC ( 5 % methanol in ethyl acetate ) afforded the title compound as a white solid.
Purification was performed on silica gel using 5 % methanol in ethyl acetate.
Eluted with 8 % methanol in ethyl acetate.
The residue was dissolved in a minimum amount of 10 % methanol in ethyl acetate.
This solid was washed with 10 % methanol in ethyl acetate to provide 96 mg of crude product.
The crude material was subjected to silica gel chromatography ( 5 % methanol in ethyl acetate ).
Purification by flash chromatography ( 3 % methanol in ethyl acetate ) afforded the title compound.
The crude black product was chromatographed on silica eluting with 40 % methanol in ethyl acetate.
The pad was eluted with 10 % methanol in ethyl acetate.
This was purified on silica, eluting with ethyl acetate, increasing to 2 % methanol in ethyl acetate.
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This was rechromatographed using a gradient of methanol in ethyl acetate ( 0 to 4 % ) as eluant.
This solid was repurified by flash silica chromatography, elution gradient 0 to 30 % methanol in ethyl acetate.
The product was eluted with 20 % methanol in ethyl acetate.
This crude material was chromatographed through 100 g of Merck silica gel using 0.2 % methanol in ethyl acetate.
Purification vía column chromatography ( SiO2, 5 % methanol in ethyl acetate ) afforded the title compounds.
The dark red oil was chromatographed on silica eluting with 20 % methanol in ethyl acetate.
Chromatography on alumina in a gradient of 3-10 % methanol in ethyl acetate afforded 2 fractions.
The reaction mixture was filtered using SPE ( silica, eluting with 30 % methanol in ethyl acetate ).
Chromatograph the residue on silica gel ( 15 % methanol in ethyl acetate ) to give the product.
This was chromatographed on alumina in a gradient of 3-15 % methanol in ethyl acetate.
The filtrate is extracted with 10 % methanol in ethyl acetate.
Purification was by chromatography eluting with 0-20 % methanol in ethyl acetate.
Flash chromatography, eluting with a gradient from 0-5 % methanol in ethyl acetate, afforded desired product.
Compound 6 was obtained as a white solid by elution with 10 % methanol in ethyl acetate.
Then the silica gel was washed with 2-4 % methanol in ethyl acetate.
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